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Volume 23 (1871) (426 pages)

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Page: of 426

236 SCIENTIFIC PRESS. {October 14, 1871.
ON THE ASSAY OF GOLD.
BY HENRY G. HANKS.
[Expressly for the Prrss.—Continued.]
When several assays of gold hnllion are to be
made together, the plan of operation is somewhat modified. Let it be reqnired to condnet
nine assays at once. Certain tools and appliances will be necessary which have not yet been
described.
A piece of hard wood is made abont four
inches sqnare and an inch in thickness. On
one side a portion of the wood projects to serve
as a haudle; nine half inch holes are bored in
the square part nearly through the thickness.
On the nnder snrface in each corner a small
knob is screwed which serves as feet to raise
the board above the table. In each of the
holes is to be placed a tnbe of glass closed at
one end. The other end is cnt off sqnare and
gronnd flat on a grind stone or emery wheel.
The sizeof thetnbes is snch that they can be easliy removed andreplacedin the holes. The tnbes
area little more than an inch long, so that they
can be easily grasped with the finger and thnmb
when it is reqnired to remove them from the
holes.
Each of the tubes are marked with a letter of
the alphabet from A to I inclnsive. “This may
be done with a writing diamond or with a corner of a freshly broken file. Near each hole is
also stamped a letter, using the same set as
those marked on the tnhes. For want of a
hetter name let this he called a ‘‘ tnbe rack.’
On commencing the assay the bars are first
to be stamped with the running nnmber of the
assays, to correspond with the entries in the
record book of the assay office. Similar entries
are then made on a small memorandnm book
and to each entry the letters are added, thns,
No. 794, A.—No. 795, B.—No. 796, C.—etc.
The bars are then all taken to the anvil and
assay chips are cnt from them, or borings taken
in the manner hefore described.
The clippings from the bar stamped 794
must be pnt into the tnbe marked ‘‘ A,” which
is then placed in its proper hole. Those of
795 in the tnhe marked ‘'B,”’ etc., etc. The
bars are then set aside and the tnbe rack taken
to the balance. Here other pieces of apparatus
will be reqnired. A sqnare block of wood with
a single hole bored in it the same size and
depth of those in the tnbe rack, and another
sqnare piece of wood with handle of the same
size and thickness as the tnbe rack; bnt instead
of holes, nine hemispherical cavities are cnt,
each of which is abont an inch in diameter, and
half aninch deep. These cavities are marked
with the same letters and in the same snccession as those of the tnbe rack.
The tnbe marked ‘‘A’’ is lifted from the rack
and placed vertically in the hole in the block,
which serves for a temporary stand forit. The
clippings that are contained in it must previonsly be ponred ont on a clean piece of paper
placed for convenience inside the balance case.
After the assays are weighed ont the remaining
gold is pnt back intothe tnhe rack. Theassays
in their leaden euvelopes are placedin the cavity
marked ‘‘A.” ‘B” is then treated in the
same way, and so on through the whole set.
Nine cnpels are then marked and placed in
the mnfile in the same order and with the same
letters. The object of marking the cnpels is,
that it is sometimes necessary to chauge their
position in the muffle. And sometimes even
to take one or more of them out, hefore the
others are finished.
The manner of niarking the cnpels is as follows: Some red chalk is gronnd fine, mixed
with water and kept in a small wide monthed
bottle for use. When it is reqnired to mark
enpels, the contents of the bottle aremixed and
apphed with a small camel's hairbrnsh. The .
enpels shonld be marked on two sides.
‘When the cnpels are taken from the mufile,
they are placed in a rack of sheet iron divided
into nine compartments, and when the bnttons
are removed they are placed back into the
cavities in the board from which they were
taken when placed in the cupels. This serves
to convey them to the balance when they are
weighed, alloyed with silver and returned to
the mufile for second cupellation. It will be
seen that to this stage the assays are always
kept in compartments hearing their mark, and
with ordinary care no mistake can ocenr.
When the assays are alloyed with silver and
rolled ont, a letter is stamped on the end of
each, somewhat deeply. The assay is then
rolled np in spiral form in the nsnal manner
commencing at the end which is not stamped.
This letter will be as distinctly seen after boiling in acid as before. The cornets are then
placed in flasks, boiled with acid and dried in
the nsnal manner.
Ithas been recommended to place all of the
cornets in one flask and after boiling, to invert
it in a somewhat capacions dish of water; to
pick ont the cornets with a pair of forceps, and .
to anneal them altogether in the mufile ona tile. .
I have never tricd it, bnt I cousider it to be un.
safe, as with the best of care the cornets are
sometimes broken in the boiling. The elegant
plan of boiling a nnmber of cornets in baskets .
of platinnm wire, in the same vessel, is open to
the same objection.
The manner of nsing the proof is as follows:
first consider what will be the average fineness
of the assays yon are condneting. Your preliminary assays will furnish yon the data. Let
it be snpposed that this average will be .950
weigh ont 950-thonsandths of pure gold, alloy
it with 2% its weight of silver and cnpel it in
the muffie with the nine assays, boil with the
same acid, and nnder exactly similar cirenmstances, heat it to redness in a dry cnpand weigh
it. It will generally be found to have increased
in weight owing to the snrcharge beingin excess
of the mechanical loss. What the proof has
gained in weight mnst be subtracted from the other assays, when many assays are to be niade from
the samé mine; an alloy of copper, silver and pure
gold mnst be made np as nearly identical as can
be with the composition of the bnilion, and this
alloy nsed asa proof. Of course a full nnit
must be employed in this case.
There are a few points to be borne in mind
in making the bnilion assay to insnre success,
The alloy of gold and silver shonld not be rolled ont too thin as it is likely to be broken when
this precantion is disregarded.
The cornet mnst never be weighed withont
being heated to redness. Simple drying will not
give correct resnlts.
In boiling with acid, .the flasks shonld be
tnrned on their sides at an inclination of 45° to
prevent loss of acid in the event of sndden ebullition.
A gradnated measnre shonld be nsed for the
acid, that the amonnt pnt in each flask shall be
equal.
Commou water shonld never be nsed in washing the cornet, as chloride of silver is formed
in the pores of the gold, which cannot be removed, and which being insolnhle in acid remains in the cornet and gives incorrect resnlts.
Gold is always weighed in Troy onnces and.
decimals. Itis best to have the onncesin decimals also. A convenient set shonld be constructed as follows:
Ounces.
500
Decimals
0,500
tested for accuracy, and compared with a standard set.
Althongh itis hetter to be provided with a
fnll set of weights and a good hnilion balance,
still it is possible to weigh very closely with a
set of 20 onnces and decimals, and a set of avordnpois ponnds on a good common balance, by
connterpoising, which has heen before described.
Each ponnd avordnpois is 14.5833 Troy onnces.
What the bar lacks of a ponnd mnst be made np
with Troy onnces and decimals. The nuniber
of ponnds is to be multiplied by the factor given
above and this snm added to the onnce weights
nsed to complete the weighing. The result will
he the weight of the bar in Troy onnces and
decimals. Of conrse the pound weights mnst
he examined and their acuracy verified.
It may sometimes be interesting to know the
relation between the fineness of gold and its
value in carats. Pure gold (1000 fine) is said
to be 24 carats fine, 12 carats wonld evidently
be 500 fine or one-half gold—all gold is so
computed in England, the standard being 22
Carats; gold of 23 carats is said to be one carat
‘better’ as 21 would be one carat ‘‘worse.”’
The following table will show the relative
valne :
0.041667
AnrrScate Compounp.—We would call
the attention of engineers and others tothe
advertisement, in another column, of
Rickard & Durden’s Anti-Scale Compound,
one of the most valuable preparations for
the purpose intended, which has ever been
presented to the public. A full notice of
this preparation was given in the ScmytTir1c Press about three months since.
A Canprpate.—Mr. Ira H. Reed, of
West Point, Calaveras Co., an old subscriber and reliable correspondent of the
Screnrivic Press, announces to us that,
although no politician, he is a candidate
for engrossing clerk of the next State
Assembly.
Removal.
The entire business office of the Scrmntric Press, Pacrrio Rurau Press, and
onr U. S. and Foreign Patenr AcENnoy
and EineRavinG establishment, has been
removed to No. 338 Montgomery street, on
the southeast corner of California street,
diagonally opposite Wells, Fargo & Co.’s.
ComBInaTIon GRAIN HarvesTeR.—B. F.
Cook, of Napa, the inventor of several interesting machines, (someof which have
been patented) has combined a Haines’
header with a Pitts’ thresher, and a portable threshing engine, whereby he cuts the
grain in the field, threshes, cleans and sacks
itin one operation. His model at the State
Fair showed the plausibility of his plan in
theory. He adjusts the machinery so that
all the work of cutting, threshing and
cleaning can be done by the power of the
engine if desired, so as to leave no work
for the teams, but to draw the machine.
He has an ingenious method of leveling
parts of the machine, whereby the engine
and bviler cau be kept constantly level
over uneven or sideling ground. Working
experiments in the field have conviuced Mr.
C. that his machine is practical, and we
hope we will find ample means to help him
demonstrate most speedily its value. His
machine is calculated to cut 18 feet wido.
© ApouT THE Loss OF QUICKSILVE RB.’
The communication under the above title,
which appears on the third page of the
present issue, found its way there through
inadvertence. The writer evidently misunderstands both the nature of the’ information asked for by Mr. Panl, and the object in seeking that information; and we
presume no miner will be so misled as to
suppose that Mr. P. has any other object
in view in seeking for the information than
the general benefit of the miners themselves.
Tur Gonpen Stare Iron Works(co-operative)are putting up a number of Stevenson’s mouldboard paus ‘of a large size, and
some eight-foot settlers, for the Metropolitan Mill and Mining Co., Eureka, Nevada.
They are also making some large hydraulic and scrow presses for the viueyards of
Eberhardt and Lachman. The castings
and condensers forthe Kuox and Osborne’s
Patent Furnace for the Pheenix Quicksilver Mine in Pope Valley, Napa Co., are
under way. ‘The men are also at work on
large quantities of White and Grey Iron }castings for stamp aud pan shoes and dies.
TInrortant Water Surr.—A suit involying the title to certain water privileges,
was decided last week by Judge Field.
The action was brought by the City of
Gold Hill Water Co. to enjoin the Cole §S.
M. Co. from certain water privileges. A
temporary injunction was allowed by the
United States Cireuit Court. The case was
subsequently heard by J udge Field, Associate Justice of the U.S. Supreme Court,
who made an order dissolving the injunction, leaving the Cole S. M. Co. in possession of their privileges.
State Fair Gold Medals,
By an advertisement in Ruran Press
it will be seen that all claimants to the
State Agricultural Society’s Gold Meadals
are required to furnish statements relative
to the manufacture or production of the
articles exhibited, and on which they claim
the award of the medal, or npon which
they base their claim of merit.
Tus San Francisco Guass Works, situated on King street near Fourth, in this
city, commenced operations again on the
12th inst. Mr. Newman, who is in charge,
informs us that everything is now in readi
ness for orders in this line.
Avertnu’s Caemican Paryt.—An advertisement of this valuable product will be
found in another column. This is the
same paint of which we gave a lengthy description in our last week’s issue,
Complete Volumes of the Scientific Pre
irom January, 1864, can be had at this office at $3 Gee
Xqiume: Bound in cloth, $5. A limited number only
on hand.
CouGHs.—THE ADMINISTRATION OF MepieraL Prep.
arations in the form of a lozenge is of all modes ths
most eligible and convenient, more especially as regards
“Brown's Bronchial Troches," or
Cough Lozenges, allay irritation which induces cough.
ing, giving instant relief in Bronchitls, Hoarseness, In.
a CoucH Rrmepy.
fluenza, and Consumptive and Asthmatic complaints.
Opera Glasses, ‘Pebble Spectacles, and
Eyeglasses, in great variety. wholesale and retnil. CG
MULLER, Optician, 205 Montgomery street, Russ Block,
San Francisco, Tv23-3m.
Scientific and Practical
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os
MINING, METALLURGY, ETC.
BY GUIDO KUSTEL
MINING ENGINEER AND METALLuRGIsT.
Published and Sold by
DEWEY & CO.
Roasting of Gold and Silver Ores, and the
Extraction of their Respective Metals without Quick.
silver. 1870.
This rare book on the treatment of gold and silver
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It contains 142 pages, embracing illustrations of furnaces, implements and workiug apparatus.
It isa work of great merit, by an author whose reputation is unsurpassed in his speciality.
Price $2.50 coin, or $3 currency, postage free.
Concentration of Ores (of all kinds), ineluding the Chlorination Process for Gold-bearing
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This work is unequaled by any other published, embracing the subjects treated. Its authority is highly
estecmced and regarded by its readers; containing, as it
does, much essential information to the Miner, Millman, Mctallurgist, and other professional workers in
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together and insimple order. It contains 120 diagrams,
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Nevada and California Processes of Silver
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full e: ions and directi for all metallurgical
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of the ingot. Also,a description of the general metallurgy of silver ores. 1864.
As its title indicates, this work gives a wide range of
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in precious metals, affording hints and assistance of excccding value to hoth the moderately informed and the
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Price, $5in cloth; $6 ln lesther—coin.
For single copies of the ahove works, or for the trade,
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DEWEY & CoO.,
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BETTS’S CAPSULE PATENTS.
To prevent INFRINGEMENTS, NOTICE IS HEREBY
GIVEN, that BETTS'S NAME is ON EVERY OAPSULE
he makes for the principal merchants in England and
¥rance, thus enabling vendor, purchaser, and consumer,
not only to identify the ennineness of the Capsule, but
likewise the contents of the vessel to which it is applied.
The Lord Chancellor, in his indement, said that the Capsnles are not used merely for the pnrpose of the ornament
but that they are perigee in protecting the wine from
injury, and insuring its genuineness.
Max BACTORIAS:—1, WHARF ROAD, CITY ROAD,
MLONDON. AND BORDEAUX, FRANCE.
J. M. STOCKMAM,
Manufacturer of
PATTERNS AND MODELS.
(Over W. T. Garratt's Brass Foundry).
Entrance, No. 129 Fremont street, San Francisco.
&y23-3m